Ix .Al 4-(sec-butyl) phenol. HMBC HO- \ CK / 9—CH3 10 J h o h 50 hioo -150 ppm |"i i 'i i i i i i i i i i i i i i i i i j i't I i i i i i-r-f-n i i i i i i i-prrrmTTTTrnttti i j, i i i i i i i i-m-m i i i i i i i ppm 6 4 2 0 Current Data Paraeeters kane PSDfeno] EXPNO 20 PHOCNO 1 F2 - Acquisition Paramet 0ate_ 951011 lime 21 04 INS1RUN spect PflOBHQ 5 TBI 113 PJL PROG lnv4Qslrne 10 2046 solvent CDC 13 NS 0 DS 4 SHH 5000.000 HI FIDflES 2.441406 HI ao 0 2048500 sec RG 4597.6 DM 100.000 usee DE 4 50 usee ie :9a. o K 01 2.50000000 sac PI 7.SO usee 06 0.06660000 sec P3 15.00 usee SF02 125 7684284 MH2 NUC2 I3C PL2 -4.00 OB DO 0.00000300 sec PI6 1000.00 usee 016 0 OOOIOOOO sec P2 15.00 usee D13 0.00000400 sec de 4 50 usee SF01 600.1322006 Muz nuci * 1M PLI •3.00 06 INO 0.00002209 sec Fl - Acquisition parame mo 2 ID 1024 sfoi 125 76B4 MHZ FIORES 22.107798 Hz sm 190.001 PPn F2 - Processing parameters 51 2049 5F 500 1300326 MHZ KM OSIME SSO 4 LB 0 00 Hz GB 0 PC 1 40 Fl - Processing paraiteters SI 1024 , MC2 Of SF 125 7577820 Wl MDM OSINE SSB 6 LB 0 00 HZ 2D «nr plot parameters CX2 15.00 cm cxi 15 00 cm F2PL0 8.000 ppn F2L0 4001 04 Hz F2PH1 -0.200 ppn F2H1 -100 03 H2 F1PL0 174.666 ppn F1L0 21965 65 Hz F1PH1 -5.000 ppn FIHI -620 79 HZ F2PPNCN 0 54667 ppn/cm F2H7CM 273.40442 HZ/CH f IPPML'N 11.97775 ppn/cm F III7CM ims.29579 HZ/cn 0.935 2.000 1.990 Ól b Čn b Ui In Ol b D u o < 1.051 1.985 in b Úl OJ b in 2.069 2.015 ■o "O 3 r" o KJ O CTI CO 13 C 1D: kys. listová 3 7 H„hL. 2 M 4 „.N O 22 O 180 160 140 120 100 80 60 40 20 ppm 1H-15N HMBC: kys. listová 52-1h (PPm) 100 150 200 250 300 50- E Q. O. O IO 100- 150- T 1H-13C HMBC: kys. listová -- —t— 8 52 - 1H (ppm)