Inroductory notes Classes Fridays 9 – 14 Credits requirements -Protocols from the practical sessions (submit et least 3 days before exam) -Exam (both theory and practice), within or outside the exam period - Supporting material On my web page http://www.ncbr.muni.cz/~fiala/ or in IS under Learning Materials Presentations Instructions for practical sessions Example protocol Questions for the exam Additional presentations eKurz CEIT_NMR_1 (practical sessions) PřF:CEIT_NMR_1 Basics of NMR spectrometer measurements (muni.cz) https://is.muni.cz/auth/el/sci/ekurzy/CEIT_NMR_1/um/ - Spectrometers Linux operating system Choice of interface – MATE recommended Software TopSpin 4 (Bruker) Free academic license after registration https://www.bruker.com/en/products-and-solutions/mr/nmr-software/topspin.html? Third party software Commercial: ACDNMR, MNOVA Free: SpinWorks, NMRPipe, matNMR 3, iNMR Notes to TopSpin 4 Currently, versions 4.1.X installed on spectrometers, 4.3 available on NMRCF datastation When you open Topspin for the first time under your own account, you need to set up a few things -Set the path to data -Create directory for your data -Create a dataset in your data directory -Open and customize the status panel -Disable zg safety -Other customizations available – colors, # of command lines, lock grid lines etc. The preferences are stored in your home directory, e.g. /home/fiala In the directory .topspin1 If you want to use someone else‘s setup, copy this directory from his/her home directory to your home directory before starting TopSpin Becaming a user After passing examination Read and follow the Operaton rules User access - Ceitec.cz User account will be created for you (Petr Padrta) You get access to the booking system Request at User access - Ceitec.cz new registration (Jaromír Tousek)