Mw = 13.8 kDa time [s] intensity R1 intensity R2 0.010 0.9858 0.9056 0.020 0.9717 0.8202 0.030 0.9579 0.7428 0.056 0.9229 0.5741 0.104 0.8615 0.3567 0.200 0.7507 0.1378 0.392 0.5701 0.0205 0.776 0.3287 0.0005 1.544 0.1093 0.0000