C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2006
Extent and Intensity
0/4/0. 4 credit(s) (fasci plus compl plus > 4). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: Thu 8:00–11:50 03016, J. Křivohlávek
C1080/02: Mon 14:00–17:50 03016, D. Dastych
C1080/03: Tue 12:00–15:50 03016, D. Dastych
C1080/04: Tue 16:00–19:50 03016, D. Dastych
C1080/05: Fri 11:00–14:50 03016, J. Křivohlávek
C1080/06: Wed 12:00–15:50 03016, J. Taraba
C1080/07: Wed 16:00–19:50 03016, J. Taraba
C1080/08: Tue 7:00–10:50 03016, M. Černík
C1080/09: Wed 7:00–10:50 03016, M. Černík
C1080/10: Fri 15:00–18:50 03016, J. Novosad
C1080/11: Fri 7:00–10:50 03016, J. Křivohlávek
C1080/12: Thu 16:00–19:50 03016, J. Pinkas
C1080/13: No timetable has been entered into IS.
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2007, Autumn 2008, Autumn 2009.
  • Enrolment Statistics (Autumn 2006, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2006/C1080