C7780 Inorganic Materials Chemistry

Přírodovědecká fakulta
podzim 2009
Rozsah
2/0/0. 2 kr. (příf plus uk plus > 4). Doporučované ukončení: zk. Jiná možná ukončení: k.
Vyučující
prof. RNDr. Jiří Pinkas, Ph.D. (přednášející)
Garance
prof. RNDr. Jiří Pinkas, Ph.D.
Ústav chemie – Chemická sekce – Přírodovědecká fakulta
Rozvrh
Út 15:00–16:50 Kontaktujte učitele
Předpoklady
Thorough knowledge of principles and facts covered by the courses of General, Inorganic, Organic, and Physical Chemistry is required.
Omezení zápisu do předmětu
Předmět je nabízen i studentům mimo mateřské obory.
Mateřské obory/plány
Cíle předmětu
This course covers the basic principles of Materials Chemistry with the emphasis on inorganic materials. The lecture focuses on the relation between structure and propertis of materials. Synthetic methods are grouped according to the physical state of reactants: solid, liquid, and gaseous. Fabrication methods of different shapes, such as fibers, thin films, and nanopaticles, are also covered.

Students will learn:
the basic principles of structural chemistry and generic structural types of solid state compounds, they will be able to apply them to other structural problems;
mechanical, thermal, optical, electric, and magnetic properties of materials in correlation to their structure and judge new materials properties;
to employ a variety of physico-chemical methods for the characterization of structure, morphlogy and properties of materials;
to understand principles of classical solid-state and new soft synthetic techniques for variety of materials;
to apply these synthetic methods to the fabrication new compounds and new morphologies;
Osnova
  • 1. Introduction, Materials Science, Materials Chemistry, Chemical Synthesis of Materials.

    2. Basic Structural Chemistry. Inorganic Structure Types. Metals, Ionic, and Covalent Compounds. Defects.

    3. Physicochemical Methods of Materials Characterization.

    4. Electronic Structure of Solids, Chemical Bonding, Band Theory.

    5. Electrical, Mechanical, Thermal, Optical, Magnetic Properties of Materials.

    6. Direct Reaction of Solids, Kinetics, Synthesis of Spinel.

    7. Carbothermal Reduction, Self-Sustaining Reactions, Combustion Reactions, Polymer Pyrolysis, Mechanochemical Synthesis, Microwave-Assisted Synthesis.

    8. Dry High-Pressure Methods, Detonation Reactions, Diamond Synthesis, Hard Materials.

    9. Vapor Phase Transport, Aerosol Routes, Flame Hydrolysis.

    10. Precursor Methods, Flux or Molten Salt Method, Ionic Liquids, Sonochemical Synthesis.

    11. Sol-Gel Methods, Hydrothermal Synthesis.

    12. Zeolites, Mesoporous Materials, Layered Materials, Intercalation.

    13. Growth of Single Crystals.

    14. Synthesis of Thin Films, Chemical Vapor Deposition, Self-Assembled Monolayers.

    15. Nanostructured Materials.
Literatura
  • SCHUBERT, Ulrich a Nicola HÜSING. Synthesis of Inorganic Materials. Weinheim: Wiley-VCH, 2000, 396 s. ISBN 3-527-29550-X. info
  • MÜLLER, Ulrich. Inorganic Structural Chemistry. 2. vyd. John Wiley & Sons., 1993. ISBN 0-471-93717-7. info
  • CALLISTER, William D., Jr. Materials Science and Engineering, An Introduction. 4. vyd. John Wiley and Sons, 1997. ISBN 0-471-13459-7. info
  • SMART, Lesley a Elaine MOORE. Solid state chemistry : an introduction. 2nd ed. London: Chapman & Hall, 1995, xiv, 379 s. ISBN 0-412-62220-3. info
  • SEGAL, David. Chemical Synthesis of Advanced Ceramic Materials. Cambridge, UK: Cambridge University Press, 1989. ISBN 0-521-35436-6. info
  • INTERRANTE, L. V. a M. J. HAMPDEN-SMITH. Chemistry of Advanced Materials, An Overview. New York: Wiley-VCH, 1998. ISBN 0-471-18590-6. info
  • BRUCE, D. W. a D. O'HARE. Inorganic Materials. Chichester: John Wiley & Sons, 1997. ISBN 0-471-96036-5. info
  • YANAGIDA, H., K. KUNIHITO, M. MIYAYAMA a H. YAMADA. The Chemistry of Ceramics. John wiley & Sons, 1996. ISBN 0-471-96733-5. info
  • HOFFMANN, Roald. Solids and Surfaces. New York: VCH Publishers, 1988. ISBN 0-89573-709-4. info
  • KODAS, T. a M. HAMPDEN-SMITH. The Chemistry of Metal CVD. Weinheim: VCH Weinheim, 1994. ISBN 3-527-29071-0. info
  • KRATOCHVÍL, Bohumil. Chemie a fyzika pevných látek 1. Praha: Vysoká škola chemicko-technologická, 1994, 233 s. ISBN 80-7080-196-4. info
  • KRATOCHVÍL, Bohumil. Základy fyziky a chemie pevných látek II. Praha: Vysoká škola chemicko-technologická, 1990, 160 s. ISBN 80-7080-055-0. info
  • MASON, Timothy J a John P LORIMER. Applied Sonochemistry. Weinheim: Wiley-VCH, 2002, 303 s. ISBN 3-527-30205-0. info
  • WEST, Anthony R. Basic Solid State Chemistry. Second Edition. Chichester: John Wiley & Sons, 1999. ISBN 0-471-987565-5. info
  • MASON, Timothy J. Sonochemistry. Oxford: Oxford University Press, 1999, 92 s. Oxford Chemistry Primers. ISBN 0-19-850371-7. info
  • GIROLAMI, Gregory S., Thomas B. RAUCHFUSS a Robert J. ANGELICI. Synthesis and technique in inorganic chemistry :a laboratory manual. 3rd ed. Sausalito, Calif.: University Science Books, 1998, xiii, 272. ISBN 0-935702-48-2. info
  • HOLZAPFEL, Wilfried B a Neil S ISAACS. High-Pressure Techniques in Chemistry and Physics. Oxford: Oxford University Press, 1997, 388 s. The Practical Approach in Chemistry Series. ISBN 0-19-855811-2. info
  • JENKINS, Ron a Robert L. SNYDER. Introduction to X-ray powder diffractometry. New York: John Wiley & Sons, 1996, xxiii, 403. ISBN 0471513393. info
  • WELLER, Mark. Inorganic Materials Chemistry. Oxford, UK: Oxford University Press, 1994. ISBN 0-19-855799-X. info
  • CHEETHAM, A K a Peter DAY. Solid State Chemistry - Compounds. Oxford: Oxford University Press, 1992, 304 s. ISBN 0-19-855166-5. info
  • CHEETHAM, A K a Peter DAY. Solid State Chemistry - Techniques. Oxford: Oxford University Press, 1987, 398 s. ISBN 0-19-855286-6. info
Výukové metody
The course taught in English. It consists of 14 lectures of 50 minutes each. Course materials, such as lecture slides, supplementary articles, tables, are available to students in the Information System of Masaryk University. Additional relevant lectures by visiting professors under INNOLEC program are part of the course in particular cases.
Metody hodnocení
There are 3 graded homeworks during the semester. At the end of the course every student will give a short presentation on a selected topic concerning materials chemistry. Written final exam worth 100 pts, minimum 50 pts to pass. Weights: final test 75%, homeworks 15%, presentation 10%.
Vyučovací jazyk
Angličtina
Navazující předměty
Informace učitele
The final exam covers the basic inorganic struture types, material properties, characterization methods, synthetic methods in solid, liquid, and gas phase as well as methods of the single crystal growth, thin film fabrication, and nanostructured materials preparation.
Další komentáře
Studijní materiály
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