C1620 General and Inorganic Chemistry - lab.

Faculty of Science
Autumn 2002
Extent and Intensity
0/2/0. 2 credit(s) (fasci plus compl plus > 4). Type of Completion: z (credit).
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
RNDr. Valerie Richterová, Ph.D. (seminar tutor)
Guaranteed by
doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C1620/01: No timetable has been entered into IS. A. Mareček
C1620/01a: No timetable has been entered into IS. A. Mareček
C1620/02: No timetable has been entered into IS. M. Alberti
C1620/02a: No timetable has been entered into IS. M. Alberti
C1620/03: No timetable has been entered into IS. M. Alberti
C1620/03a: No timetable has been entered into IS. M. Alberti
C1620/04: No timetable has been entered into IS. M. Alberti
C1620/04a: No timetable has been entered into IS. M. Alberti
C1620/05: No timetable has been entered into IS. D. Dastych
C1620/05a: No timetable has been entered into IS. D. Dastych
C1620/06: No timetable has been entered into IS. V. Richterová
C1620/06a: No timetable has been entered into IS. V. Richterová
C1620/07: No timetable has been entered into IS. V. Richterová
C1620/07a: No timetable has been entered into IS. V. Richterová
C1620/08: No timetable has been entered into IS. V. Richterová
C1620/08a: No timetable has been entered into IS. V. Richterová
Prerequisites
NOW( C1601 General and Inorg. Chemistry )
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
This course covers basic laboratory operations (filtration, crystallization, distillation, extraction, sublimation, volumetric methods), syntheses of simple inorganic compounds as well as determination of physicochemical constants of compounds.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for laboratory work and writing reports, safety rules. Pass-requirements. 2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. 3. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Heating, cooling, stirring. Filtration, simple distillation, heating under reflux, sublimation, Soxhlet extraction. Gas and liquid volume measurements, Balances and weighing.Melting point measurement. 4. Synthesis of the KAl(SO4)2.12H2O. Crystalization. 5. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture. 6. Extraction of the PbI2 from PbI2 and PbCrO4.PbO mixture. 7. Sublimation of the 1-acetamidoadamantane, melting point measurement. Preparation of 0,5 M H2SO4. Volumetric measurement of the molarity of H2SO4. 8. Final test, glassware and laboratory cleaning.
Literature
  • MAREČEK, Aleš and Antonín RŮŽIČKA. Laboratorní technika pro nechemické obory. 1. vyd. Brno: Vydavatelství Masarykovy univerzity, 1997, 44 s. ISBN 8021016531. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá jednou za dva týdny. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011 - acreditation.
  • Enrolment Statistics (Autumn 2002, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2002/C1620