C1620 General and Inorganic Chemistry - lab.

Faculty of Science
Autumn 2008
Extent and Intensity
0/2/0. 2 credit(s) (fasci plus compl plus > 4). Type of Completion: z (credit).
Teacher(s)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Ing. Lubomír Prokeš, Ph.D. (seminar tutor)
RNDr. Richard Ševčík, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Guaranteed by
doc. Mgr. Marek Nečas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C1620/01: Thu 9:00–12:50 C10/316, M. Nečas
C1620/02: Thu 9:00–12:50 C10/316, M. Nečas
C1620/03: Thu 14:00–17:50 C10/316, L. Prokeš
C1620/04: Thu 14:00–17:50 C10/316, L. Prokeš
C1620/05: Fri 8:00–11:50 C10/316, L. Prokeš
C1620/06: Fri 8:00–11:50 C10/316, L. Prokeš
C1620/07: Mon 14:00–17:50 C10/316, R. Ševčík
C1620/08: Mon 14:00–17:50 C10/316, R. Ševčík
C1620/09: Mon 9:00–12:50 C10/316, R. Ševčík
C1620/10: Mon 9:00–12:50 C10/316, R. Ševčík
Prerequisites
NOW( C7777 Handling chemicals )
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 16 fields of study the course is directly associated with, display
Course objectives
This course aims to introduce students to basic laboratory operations (filtration, crystallization, distillation, extraction, sublimation, volumetric methods), syntheses of simple inorganic compounds as well as determination of physicochemical constants of compounds.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for laboratory work and writing reports, safety rules. Pass-requirements.Balances and weighing.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    3. 4. Synthesis of the KAl(SO4)2.12H2O. Crystalization.

    5. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    6. Extraction of the PbI2 from PbI2 and PbCrO4.PbO mixture. 0.5M NaOH factor determination.

    7. Sublimation of the 1-acetamidoadamantane, melting point measurement. Preparation of 0,5 M H2SO4. Volumetric measurement of the molarity of H2SO4.
Literature
  • MAREČEK, Aleš and Antonín RŮŽIČKA. Laboratorní technika pro nechemické obory. 1. vyd. Brno: Vydavatelství Masarykovy univerzity, 1997, 44 s. ISBN 8021016531. info
Assessment methods
Credits are awarded if: (1) each laboratory exercises is completed; (2) student can show an understanding of each completed laboratory exercise and related principles and calculations (stoichiometry, concentrations, titrations); (3) laboratory reports to all exercises are submitted and approved by the teacher.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2009, Autumn 2010, Autumn 2011 - acreditation.
  • Enrolment Statistics (Autumn 2008, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2008/C1620