C1635 Analytical chemistry - laboratory course

Faculty of Science
Autumn 2006
Extent and Intensity
0/4. 4 credit(s) (fasci plus compl plus > 4). Type of Completion: z (credit).
Teacher(s)
Mgr. Jiří Machát, Ph.D. (seminar tutor)
Guaranteed by
Mgr. Jiří Machát, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Timetable
Thu 14:00–17:50 Cpd,01004
  • Timetable of Seminar Groups:
C1635/01: No timetable has been entered into IS.
Prerequisites (in Czech)
NOW( C1660 Basic Analytical Chemistry )
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 12 fields of study the course is directly associated with, display
Course objectives
Basic laboratory course of analytical chemistry -qualitative analysis, gravimetric analysis, volumetric analysis: acidimetric, redox, chelatometric. Instrumental analysis: potenciometric titration with glass, platinum and silver electrodes. Spectrophotometry. Chemometrics.
Syllabus
  • QUALITATIVE ANALYSIS 1. Analytical reactions of kations I.A, II.A and NH4+. 2. Analytical reactions of kations Pb, Cu, Fe, Co, Ni, Mn, Zn, Al. Analysis of mixture. 3. Analytical reactions of anions Cl-, SO42-, PO43-, NO3-, CO32-, B(OH)4-. Qualitative analysis of unknown sample. QUANTITATIVE ANALYSIS 4. Gravimetric determination of Fe3+ as Fe2O3. 5. Alkalimetry. Standardization of 0,1 mol.l-1 NaOH volumetric solution by oxalic acid. Determination of acetic acid. 6. Manganometry. Standardization of 0,02 mol.l-1 KMnO4 and 0,1 mol.l-1 Fe (II). Determination of nitrite by indirect titration. 7. Chelatometry. Standardization of 0,05 mol.l-1 EDTA by Pb(NO3)2. Determination of Ni, titration of Ca and Mg in mixture. 8. Spectrophotometry. Determination of Fe3+ by sulfosalicylic acid. Absorption curve, calibration graph. 9. Standardization of volumetric solution 0,l mol.l-1 NaOH by oxalic acid with potentiometric indication. Titration of acetic acid. 10. Potentiometric titration of phosphoric acid by 0,l mol.l-1 NaOH, derivation of titration curve. 11. Potentiometric redox titration. Manganometric determination of Fe (II). Titration curve for different concentration of volumetric solution. 12. Potentiometric praecipitation titration. Argentometric determination of Cl- and I- in mixture. 13. Demonstration of instrumental analytical techniques (AAS, ICP, LC, GC, CE, MS aj.)
Literature
  • OTRUBA, Vítězslav and Jaroslav ŠENKÝŘ. Základní úlohy z analytické chemie pro biology (Basic excercises of analytical chemistry for biologists). první. Brno: Masarykova univerzita, 2000, 40 pp. ISBN 80-210-2462-3. info
Assessment methods (in Czech)
Závěrečné hodnocení - zápočet. Požadavky pro udělení zápočtu - odevzdané a vyučujícím odsouhlasené protokoly ze všech absolvovaných úloh. Účast na výuce povinná, povolena 1 omluvená neúčast.
Language of instruction
Czech
Further Comments
Study Materials
The course can also be completed outside the examination period.
The course is taught annually.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2007, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Autumn 2016, autumn 2017, Autumn 2018, Autumn 2019, Autumn 2020, autumn 2021, Autumn 2022, Autumn 2023, Autumn 2024.
  • Enrolment Statistics (Autumn 2006, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2006/C1635