C3060 Organic Chemistry - laboratory course

Faculty of Science
Autumn 2007
Extent and Intensity
0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).
Teacher(s)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
RNDr. Stanislav Man, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Guaranteed by
RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: RNDr. Slávka Janků, Ph.D.
Timetable
Mon 7:00–13:50 C10/109, Wed 10:00–16:50 C10/109, Fri 10:00–16:50 C10/109
  • Timetable of Seminar Groups:
C3060/01: No timetable has been entered into IS. S. Janků
C3060/02: No timetable has been entered into IS. S. Janků
C3060/03: No timetable has been entered into IS. S. Man
C3060/04: No timetable has been entered into IS. J. Literák
C3060/05: No timetable has been entered into IS. A. Pálková
C3060/06: No timetable has been entered into IS. A. Pálková
Prerequisites
C1080; You have to pass tests of your knowledge.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 25 fields of study the course is directly associated with, display
Course objectives
Fundamental laboratory methods of organic chemistry for synthesis (heating, stirring, cooling, introduction of gases, working with decrease of pressure, drying) and separation of organic compounds (filtering, crzstallization, distillation, extraction). The methods are trained an the compounds synthesis of important types of organic reactions. The products are characterized bz melting point, thin-layer chromathography, refractive index, and infra-red spectroscopy.
Syllabus
  • 1. a) Ethylbromid (mechanismus SN2, destilace) 3. Nitrace fenolu (mechanismus SEAr, destilace s vodní parou, rekrystalizace) 4. Azobenzen (elektrochemická redukce, rekrystalizace, TLC) 5. Ethylenacetal ethylesteru 3-oxobutanové kyseliny (mechanismus AN na karbonylovou skupinu, azeotropní a vakuová destilace, práce s rotační vakuovou odparkou ) 6. a) Ethylenacetal 4,4-difenyl-4-hydroxy-2-butanonu (mechanismus AN na karbonylovou skupinu, extrakce, práce s rotační vakuovou odparkou, rekrystalizace ) b) 4,4-Difenyl-4-hydroxy-2-butanon (kysele katalyzovaná hydrolýza acetalů, extrakce, práce s rotační vakuovou odparkou, rekrystalizace) 7. 3-Nitroacetofenon (mechanismus SEAr, rekrystalizace, IČ spektrum) 8.b) 3-Aminoacetofenon (selektivní redukce, extrakce, rekrystalizace, IČ spektrum) 9. Pinakol (redukce kovem v bezvodém nepolárním prostředí, práce s rotační vakuovou odparkou) 10. Kyselina benzoová (AN na dvojnou vazbu, práce s bezvodým rozpouštědlem, extrakce, sublimace) 11. Kyselina anthranilová (Hofmannovo odbourávání amidů, rekrystalizace) 12. Ethyl-acetát (esterifikace, destliace) 13. 2-Hydroxy-5-methyl-2'-nitroazobenzen (diazotace a kopulace, rekrystalizace, TLC) 15. Kyselina 2-chlorbenzoová (diazotace a Sandmayerova reakce, rekrystalizace)
Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
Assessment methods (in Czech)
Laboratorní cvičení ukončené klasifikovaným zápočtem.
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
The course is taught annually.
General note: Vyučují učitelé katedry organické chemie.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation.
  • Enrolment Statistics (Autumn 2007, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2007/C3060