G8601 X-ray diffractometry

Faculty of Science
Autumn 2023
Extent and Intensity
1/1/0. 3 credit(s). Type of Completion: zk (examination).
Teacher(s)
Mgr. Dalibor Všianský, Ph.D. (lecturer)
doc. Mgr. Jan Cempírek, Ph.D. (lecturer)
Mgr. Kateřina Streitová (assistant)
Mgr. Lenka Skřápková (assistant)
Guaranteed by
doc. Mgr. Jan Cempírek, Ph.D.
Department of Geological Sciences – Earth Sciences Section – Faculty of Science
Contact Person: Ing. Jana Pechmannová
Supplier department: Department of Geological Sciences – Earth Sciences Section – Faculty of Science
Timetable
Tue 13:00–13:50 Gp,02006, Tue 14:00–14:50 Gp,02006
Prerequisites
! G8600 RTG-difraktometry && ! G8601k X-ray diffractometry &&!NOW( G8601k X-ray diffractometry ) && ((!(PROGRAM(B-GE)||PROGRAM(N-GE)||PROGRAM(D-GE4)||PROGRAM(D-GE)||PROGRAM(C-CV))) || (NOW( G0101 Occupational healt and safety )&&NOW( C7777 Handling chemical substances )))
knowledge from G1061 Mineralogie
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
The optional lecture for the students oriented to the mineralogy and technical mineralogy and petrology. The lecture introduces with usual X-ray powder and monocrystal methods and presents the convenient or inappropriate methods for the different problems solution. Accessible software and methods of evaluation of difractograms are described.
Learning outcomes
After finishing the course, student will be able to:
- properly prepare samples for XRD analysis;
- define requirements for data measurement and diffractometer settings;
- process, interpret, and present XRD data
Syllabus
  • The lecture consists of the parts as follows: - theory - powder X-ray diffractometry - monocrystal X-ray diffractometry - practical lessons - excursionf to XRD labs
Literature
  • International tables for crystallography. Edited by Mois I. Aroyo. Sixth edition. Chichester: Wiley, 2016, xxi, 873. ISBN 9780470974230. info
  • Modern diffraction methods. Edited by Eric J. Mittemeijer - Udo Welzel. Weinheim: Wiley-VCH Verlag GmbH & Co. KGaA, 2013, xxvi, 528. ISBN 9783527322794. info
  • WILL, Georg. Powder diffraction : the Rietveld method and the two stage method to determine and refine crystal structures from powder diffraction data. Berlin: Springer, 2006, ix, 224. ISBN 3540279857. info
  • BLOSS, Donald F. Crystallography and crystal chemistry : an introduction. 2nd print. Washington: Mineralogical Society of America, 1994, 454 s. ISBN 0030851556. info
  • Difrakcia na polykryštalických látkach. Edited by L. Smrčok. Bratislava: R & D Print, 1994, 458 s. ISBN 80-85488-01-9. info
  • JOHAN, Zdeněk, Robert ROTTER and Ervín SLÁNSKÝ. Analýza látek rentgenovými paprsky. Vyd. 1. Praha: SNTL - Nakladatelství technické literatury, 1970, 257 s. URL info
Teaching methods
periodic weekly lectures
Assessment methods
written exam
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
The course is taught once in two years.
Information on the per-term frequency of the course: Bude otevřeno v podzimním semestru 2023/2024.
Teacher's information
weekly lectures
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2002, Autumn 2003, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2009, Autumn 2011 - acreditation, Autumn 2013, Autumn 2015, autumn 2017, Autumn 2019, autumn 2021.
  • Enrolment Statistics (recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2023/G8601