C3120 Analytical Chemistry I-laboratory course

Faculty of Science
Spring 2003
Extent and Intensity
0/0/4. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Mgr. Miloš Halúzka (seminar tutor)
prof. RNDr. Přemysl Lubal, Ph.D. (seminar tutor)
prof. Mgr. Jan Preisler, Ph.D. (seminar tutor)
doc. Mgr. Petr Táborský, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Přemysl Lubal, Ph.D.
Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C3120/Ca23: No timetable has been entered into IS.
C3120/Ca24: No timetable has been entered into IS.
C3120/Ca25: No timetable has been entered into IS.
C3120/Ca26: No timetable has been entered into IS.
C3120/Ca27: No timetable has been entered into IS.
C3120/Ca28: No timetable has been entered into IS.
Prerequisites (in Czech)
Předpokladem je absolvování základních přednášek z Obecné chemie (C1020), Anorganické chemie I (C1061), Anorganické chemie II (C2062), Organické chemie I (C2021), Organické chemie II (C3022) a příslušných laboratorních cvičení z těchto předmětů.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 17 fields of study the course is directly associated with, display
Course objectives
A systematic training of "classical" analytical chemistry for students of chemistry. The course includes qualitative analysis, gravimetric analysis, and titrimetry.
Syllabus
  • QUALITITATIVE ANALYSIS
  • 1. Analytical reactions of Li(I), Na(I), K(I), NH4+, Mg(II), Ca(II), Sr(II), Ba(II).
  • 2. Analytical reactions of Hg2(II), Ag(I), Pb(II), Hg(II), Cu(II), Cd(II), Bi(III), Sb(III), Sn(II), Sn(IV).
  • 3. Analytical reactions of Al(III), Cr(III), Fe(III), Fe(II), Mn(II), Zn(II), Co(II), Ni(II).
  • 4. Analytical reactions of sulphates, sulphites, thiosulphates, fluorides, silicates.
  • 5. Analytical reactions of chromates, phosphates, arsenates, arsenites, borates, carbonates.
  • 6. Analytical reactions of chlorides, bromides, iodides, thiocyanates, hydrogensulfides, nitrites, nitrates, perchlorates. QUANTITATIVE ANALYSIS
  • 7. GRAVIMETRY: Iron determination as Fe2O3.
  • 8. ACID-BASE TITRATIONS: Standardization of standard solutions. a) Standardization of 0,1 M NaOH solution using dihydrate of oxalic acid (fft and mo with CaCl2). b) Standardization of 0,1 M HCl solution using sodium carbonate.
  • 9. ACID-BASE TITRATIONS: Alkalimetry. a) Acetic acid determination. b) Phosphoric acid determination.
  • 10. ACID-BASE TITRATIONS: Acidimetry. a) Ammonia determination. b) Sodium carbonate determination in technical liquor. c) Determination of insoluble carbonate.
  • 11. CHELATOMETRIC TITRATIONS: a) Standardization of 0,05 M EDTA solution using lead nitrate. b) Ni(II) determination. c) Determination of Ca(II) a Mg(II) cations in mixture.
  • 12. REDOX TITRATIONS: Iodometry. a) Standardization of 0,05 M Na2S2O3 solution using KIO3. b) Winkler determination of dissolved oxygen in waters.
  • 13. REDOX TITRATIONS: Bischromatometry. a) Preparation of K2Cr2O7 standard solution. b) Fe(II) determination.
Literature
  • ŠENKÝŘ, Jaroslav. Kvalitativní analýza : vybrané postupy k důkazu iontů. 2. vyd. Brno: Vydavatelství Masarykovy univerzity, 1995, 76 s. ISBN 8021011726. info
  • ŠENKÝŘ, Jaroslav. Kvantitativní analýza : pracovní návody pro základní cvičení. 1. vyd. Brno: Vydavatelství Masarykovy univerzity, 1995, 44 s. ISBN 8021012145. info
  • Kotuček M., Skopalová J., Příklady z analytické chemie, Vydavatelství UniverzityPalackého Olomouc 1997
Assessment methods (in Czech)
praktická laboratorní cvičení
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry analytické chemie.
The course is also listed under the following terms Autumn 1999, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2000, Autumn 2001, Spring 2004, Spring 2005, Spring 2006, Spring 2007, Spring 2008, Spring 2009, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.
  • Enrolment Statistics (Spring 2003, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2003/C3120