C6250 Instrumental analysis

Faculty of Science
Spring 2011 - only for the accreditation
Extent and Intensity
0/0/5. 5 credit(s) (plus extra credits for completion). Type of Completion: graded credit.
Teacher(s)
RNDr. Marta Farková, CSc. (seminar tutor)
Ing. Blanka Vrbková, Ph.D. (seminar tutor)
Guaranteed by
RNDr. Marta Farková, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
C5241 Analysis of Org.Compounds I
C2021 - Organic chemistry
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
The aim of the course is practical introduction to classical procedures of organic compounds analysis, which are the basis of instrumental methods, and to instrumental separation techniques suitable for analysis of organic compounds.
Syllabus
  • 1. Orientation tests, qualitative elemental analysis, classification and group reactions, physical constants determination of organic compounds. 2. Semimicrodetermination of carbon and hydrogen. 3. Volumetric determination of nitrogen according to Dumas and Dubsky. 4. Microdetermination of sulphur according to Schöniger. 5. Derivatization of alcohols and their identification by TLC. 6. Interpretation of spectra of organic molecules. 7. Gas chromatography. Determination of alcohols in an alcoholic drink. 8. Capillary electrophoresis. Determination of caffeine and acetylsalicylic acid in Acylcoffin. 9. Liquid chromatography on reverse phase with UV-VIS detection
Literature
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin. 1. vyd. Olomouc: Univerzita Palackého, 1981, 235 s. info
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin b. 1. vyd. Olomouc: Univerzita Palackého, 1981, 235 s. info
Teaching methods
Type of education: students have to pass all exercises included in the course
Assessment methods
Type of exam: written tests, final test, oral examination during the lessons. Students have to submit all protocols.
Language of instruction
Czech
Further Comments
Course is no more offered.
The course is taught: every week.
Teacher's information
http://www.chemi.muni.cz/~pazourek/student/oa.html
The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2000, Spring 2001, Spring 2002, Spring 2003, Spring 2004, Spring 2005, Spring 2006, Spring 2007, Spring 2008, Spring 2009, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2024, Spring 2025.