C8953 NMR - Strukturní analýza - seminář

Faculty of Science
Spring 2013
Extent and Intensity
0/1/0. 1 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
Teacher(s)
Mgr. Jan Novotný, Ph.D. (seminar tutor)
Mgr. Matúš Durec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Contact Person: prof. RNDr. Radek Marek, Ph.D.
Supplier department: National Centre for Biomolecular Research – Faculty of Science
Timetable
Wed 14:00–14:50 C04/211
Prerequisites
C8950 NMR Structural Analysis || NOW( C8950 NMR Structural Analysis )
successful completion/simultaneous registration of C8950
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
At the end of the course students should be able to: analyse and interpret 1D and 2D NMR spectra; solve the structure of an unknown compound based on the spectral analysis.
Syllabus
  • Interpretation: 1. H-1 NMR spectra. 2. C-13 NMR spectra. 3. APT. 4.+5. 1D NOE and NOESY. 6. COSY. 7. TOCSY. 8. HSQC. 9. HMBC. 10.+11. Set of spectra for one sample. 12. Presentation of group project.
Literature
    recommended literature
  • CLARIDGE, Timothy D. W. High-resolution NMR techniques in organic chemistry. 1st ed. Amsterdam: Pergamon, 1999, xiv, 382 s. ISBN 0-08-042798-7. info
  • BREITMAIER, Eberhard. Structure elucidation by NMR in organic chemistry : a practical guide. Translated by Julia Wade. Chichester: John Wiley & Sons, 1993, 265 s. ISBN 0471933813. info
  • FRIEBOLIN, Horst. Basic one- and two-dimensional NMR spectroscopy. Translated by Jack K. Becconsall. 5th completely rev. and upda. Weinheim: Wiley-VCH, 2011, xxiv, 418. ISBN 9783527327829. info
Teaching methods
Practical exercises in interpreting the NMR spectra; disscussions; group project.
Assessment methods
Participation on practical sessions, final project.
Language of instruction
Czech
Follow-Up Courses
Further Comments
Study Materials
The course is taught annually.
The course is also listed under the following terms Spring 2011 - only for the accreditation, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2024, Spring 2025.
  • Enrolment Statistics (Spring 2013, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2013/C8953