C6860 Modern Methods of Pollutant Analysis

Faculty of Science
Spring 2006
Extent and Intensity
2/0/0. 2 credit(s) (plus extra credits for completion). Recommended Type of Completion: zk (examination). Other types of completion: k (colloquium).
Teacher(s)
prof. RNDr. Jana Klánová, Ph.D. (lecturer)
prof. RNDr. Josef Komárek, DrSc. (lecturer)
Guaranteed by
prof. RNDr. Ivan Holoubek, CSc.
RECETOX – Faculty of Science
Contact Person: prof. RNDr. Jana Klánová, Ph.D.
Timetable
Mon 11:00–12:50 kamenice
Prerequisites
C6110 course, Environmental Analytical Chemistry or an equivalent should be passed.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 23 fields of study the course is directly associated with, display
Course objectives
Aim of the course is an enhancement of knowledges acquired in course C6110, Environmental Analytical Chemistry. Part engaged in organic contaminants (A. Hrdlička) deals mainly with contemporary techniques of sample preparation and with techniques hyphenating high performance separation with specific detection. Treatment of environmental samples with various matrices is discussed. In the part on inorganic contaminants (J. Komárek) requirements for trace inorganic analysis are introduced and, further, flow injection analysis, speciation of elements by electrochemical methods and by gas chromatography, applications of liquid chromatography and other techniques are discussed.
Syllabus
  • Part A: ORGANIC POLLUTANTS (by A. Hrdlička) A.I. Specific problems of organic pollutants analysis. A.II. Contemporary techniques of sample preparation. Automatized Soxhlet extraction, MAE, ASE, SFE, SPE, SPME, molecular imprints. Cloud-point extraction and polymer mediated extraction. Headspace, purge&trap. Membrane separations. Recovery estimation. A.III. Preparation of water, sediment, soil, and biota samples. Automation, on-line techniques. Multiresidual schema. Direct methods. A.IV. Hyphenated techniques: GC/FTIR, LC/FTIR, GC/OES, GC/AED, HPLC/NMR. Part B: INORGANIC POLLUTANTS (by J. Komárek) B.I. Trace inorganic analysis, practical aspects. B.II. Flow analysis, instrumentation, preconcentration. B.III. Electrochemical techniques for element speciation, ASV, electrodeposition, electrodes. B.IV. Speciation of elements by GC. Derivatization, termic desorption, detection means. Sample preparation. B.V. HPLC application, ion chromatography, GPC. Detection means. B.VI. Other techniques, LIDAR.
Literature
  • BARCELÓ, D. Environmental Analysis. Techniques, Applications and Quality Assurance. Amsterdam: Elsevier, 1993. Techniques & Instrumentation Anal. Chem., Vol. 13. ISBN 0-444-89648-1. info
  • BUFFINGTON, R. GC-Atomic Emission Spectroscopy Using Microwave Plasmas. Avandale, USA: Hewlett-Packard, 1988. ISBN 05921-90100. info
  • KALOUS, Vítěz. Metody chemického výzkumu. 1. vyd. Praha: SNTL - Nakladatelství technické literatury, 1987, 430 s. URL info
  • LOPEZ-AVILA, V. Sample Preparation for Environmental Analysis. Critical Reviews in Analytical Chemistry. 1999, vol. 29, No 3, p. 195-230. ISSN 1040-8347. info
Assessment methods (in Czech)
přednášky, ústní zkouška
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
General note: Navazuje na předmět C6110 Anal. chemie živ. prostředí.
The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Spring 2000, Spring 2001, Spring 2002, Spring 2003, Spring 2004, Spring 2005, Spring 2007, Spring 2008, Spring 2009, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019.
  • Enrolment Statistics (Spring 2006, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2006/C6860