PřF:C8953 NMR Structural Analysis - sem. - Course Information
C8953 NMR Structural Analysis - seminar
Faculty of ScienceSpring 2024
- Extent and Intensity
- 0/2/0. 2 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
- Teacher(s)
- Mgr. Jan Novotný, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor) - Guaranteed by
- prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Contact Person: Mgr. Jan Novotný, Ph.D.
Supplier department: National Centre for Biomolecular Research – Faculty of Science - Timetable
- Mon 19. 2. to Sun 26. 5. Wed 15:00–16:50 C04/211
- Prerequisites
- C8950 NMR Structural Analysis || NOW( C8950 NMR Structural Analysis )
successful completion/simultaneous registration of C8950 - Course Enrolment Limitations
- The course is also offered to the students of the fields other than those the course is directly associated with.
- fields of study / plans the course is directly associated with
- Inorganic Chemistry (Eng.) (programme PřF, D-CH4)
- Inorganic Chemistry (programme PřF, N-CH)
- Biophysical Chemistry (programme PřF, B-CH)
- Biochemistry (programme PřF, D-BCH4)
- Biochemistry (programme PřF, N-BCH)
- Biomolecular Chemistry (programme PřF, D-BCH4)
- Biomolecular Chemistry (programme PřF, N-BCH)
- Physical Chemistry (Eng.) (programme PřF, D-CH4)
- Physical Chemistry (programme PřF, D-CH4)
- Physical Chemistry (programme PřF, N-CH)
- Materials Chemistry (programme PřF, D-CH4)
- Organic Chemistry (Eng.) (programme PřF, D-CH4)
- Organic Chemistry (programme PřF, D-CH4)
- Organic Chemistry (programme PřF, N-CH)
- Structural Chemistry (programme PřF, N-CH)
- Course objectives
- At the end of the course students should be able to: analyse and interpret 1D and 2D NMR spectra; solve the structure of an unknown compound based on the spectral analysis.
- Learning outcomes
- Student will be able to:
- interpret 1D and 2D NMR spectra;
- understand and apply logical steps of structural analysis. - Syllabus
- Interpretation: 1. H-1 NMR spectra. 2. C-13 NMR spectra. 3. APT. 4.+5. 1D NOE and NOESY. 6. COSY. 7. TOCSY. 8. HSQC. 9. HMBC. 10.+11. Set of spectra for one sample. 12. Presentation of group project.
- Literature
- recommended literature
- CLARIDGE, Timothy D. W. High-resolution NMR techniques in organic chemistry. 1st ed. Amsterdam: Pergamon, 1999, xiv, 382 s. ISBN 0-08-042798-7. info
- BREITMAIER, Eberhard. Structure elucidation by NMR in organic chemistry : a practical guide. Translated by Julia Wade. Chichester: John Wiley & Sons, 1993, 265 s. ISBN 0471933813. info
- FRIEBOLIN, Horst. Basic one- and two-dimensional NMR spectroscopy. Translated by Jack K. Becconsall. 5th completely rev. and upda. Weinheim: Wiley-VCH, 2011, xxiv, 418. ISBN 9783527327829. info
- BRAUN, Siegmar, Hans-Otto KALINOWSKI and Stefan BERGER. 150 and more basic NMR experiments : a practical course. 2nd exp. ed. Weinheim: Wiley-VCH, 1998, 595 s. ISBN 3527295127. info
- Teaching methods
- Practical exercises in interpreting the NMR spectra; disscussions; group project.
- Assessment methods
- Participation on practical sessions, final project.
- Language of instruction
- Czech
- Follow-Up Courses
- Further Comments
- Study Materials
The course is taught annually.
- Enrolment Statistics (Spring 2024, recent)
- Permalink: https://is.muni.cz/course/sci/spring2024/C8953