PřF:C7021 Separation Methods - Course Information

C7021 Separation Methods

Extent and Intensity

2/0/0. 2 credit(s) (fasci plus compl plus > 4). Recommended Type of Completion: zk (examination). Other types of completion: k (colloquium).

Teacher(s)

doc. Mgr. Jan Havliš, Dr. (lecturer)
doc. RNDr. Bc. Jiří Pazourek, Ph.D. (lecturer)

Guaranteed by

doc. RNDr. Milan Dressler, CSc.
Chemistry Section – Faculty of Science

Prerequisites

C3100 + C4050 Analytical chemistry (at least C1660)

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basics of analytical separation methods, transit from liquid-liquid extraction to chromatography. Theory and praxis of Gas chromatography (GC). Efficiency of separation methods. Ion exchange chromatography. Sample preparation for analytical separation.

Syllabus

• Principles of gas chromatography, diffusion in gas phase, description of compound distribution between phases and character of compounds interaction in stationary and mobile phases. The influence of temperature and pressure of gas characteristics in gas chromatography: van Deemter theory. Basic components of gas chromatograph, sample injection. Thermo conductivity detection in gas chromatography (katharometer). Flame ionization detection (FID). Electron capture detector (ECD). Photoionization detector, conductivity detector. Types of columns in gas chromatography, stationary phase support. Capillary columns in gas chromatograhy, influence of inner diameter of capillary and the film thickness on separation. Adsorption gas chromatography - common adsorbents. Adsorbed and covalently bonded stacionary phases in gas chromatography - their properties, preparation and selection. Requirements for gas chromatography columns. Gas chromatography with programmed temperature - purpose, temperature influence on separation and characterization of retention. Hyphenation of gas chromatography with mass spectroscopy - advantages and applications. Areas of applications and examples of applications of gas chromatography. Head space analysis. Ionic compounds separation - principles. Ion exchange chromatography (IEC). Ionexes. Ion compounds separation - applications. Dionex system. Head space analysis. Supercritical fluid chromatography (SFC). Sample preparation. Thin Layer chromatography (TLC). Efficiency of separation methods. Liquid-liquid extraction. Accelerated solvent extraction (ASE). Microwave extraction.. Solid phase extraction (SPE). Solid phase microextraction (SPME). Supercritical fluid extraction (SFE).

Literature

• CHURÁČEK, Jaroslav. Analytická separace látek. 1. vyd. Praha: Státní nakladatelství technické literatury, 1990, 384 s. ISBN 80-03-00569-8. info
• POPL, Milan and Jaroslav KUBÁT. Separace látek. 3. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 1986, 171 s. info
• SOMMER, Lumír. Základy teorie analytické chemie. 1. vyd. Praha: Státní pedagogické nakladatelství, 1985, 250 s. info
• SOMMER, Lumír. Základy teorie analytické chemie. 1. vyd. Praha: Státní pedagogické nakladatelství, 1990, 138 s. ISBN 8021001070. info
• SOMMER, Lumír. Základy teorie analytické chemie. 1. vyd. Praha: Státní pedagogické nakladatelství, 1991, 185 s. ISBN 8021002158. info
• Separační metody - Plynová chromatografie

Assessment methods (in Czech)

přednáška Zk

Language of instruction

Czech

Follow-Up Courses

• C8022 Separation Methods B

Further Comments

The course can also be completed outside the examination period.
The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C8022 Separation Methods B
  C7021  

Teacher's information

http://www.chemi.muni.cz/~pazourek/student/sepmetody.html

• Enrolment Statistics (Autumn 2003, recent)
  
• Permalink: https://is.muni.cz/course/sci/autumn2003/C7021