C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2007 - for the purpose of the accreditation
Extent and Intensity
0/0/1. 1 credit(s). Type of Completion: z (credit).
Teacher(s)
Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Prerequisites
Basic knowledge of NMR spectroscopy.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.
Syllabus (in Czech)
  • 1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.
Literature
  • Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
  • Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5
Assessment methods (in Czech)
Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.
Language of instruction
Czech
Follow-Up Courses
Further Comments
The course is taught each semester.
The course is taught: in blocks.
Teacher's information
http://www.chemi.muni.cz/nmr/radek/C7998/
The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.