PřF:C7998 Basics of Experimental NMR Spe - Course Information
C7998 Basics of Experimental NMR Spectroscopy
Faculty of ScienceSpring 2011 - only for the accreditation
- Extent and Intensity
- 0/0/1. 1 credit(s). Type of Completion: z (credit).
- Teacher(s)
- Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor) - Guaranteed by
- prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science - Prerequisites
- Basic knowledge of NMR spectroscopy.
- Course Enrolment Limitations
- The course is also offered to the students of the fields other than those the course is directly associated with.
- fields of study / plans the course is directly associated with
- Chemistry (programme PřF, M-CH)
- Chemistry (programme PřF, B-CH)
- Organic Chemistry (programme PřF, D-CH)
- Organic Chemistry (programme PřF, N-CH)
- Organic Chemistry (programme PřF, N-CH3)
- Course objectives
- At the end of the course students should be able to measure of 1D NMR spectra (1H, 13C, APT) at 300 MHz spectrometer; probehead exchange; temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed in controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F). - Syllabus
- 1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.
- Literature
- recommended literature
- Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
- Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5
- Teaching methods
- Laboratory training
- Assessment methods
- Practical sessions. Practical exam.
- Language of instruction
- Czech
- Follow-Up Courses
- Further Comments
- The course is taught each semester.
The course is taught: in blocks. - Teacher's information
- http://www.chemi.muni.cz/nmr/radek/C7998/
- Enrolment Statistics (Spring 2011 - only for the accreditation, recent)
- Permalink: https://is.muni.cz/course/sci/spring2011-onlyfortheaccreditation/C7998