C5160 Physical chemistry - laboratory course

Faculty of Science
Autumn 2013
Extent and Intensity
0/0/5. 6 credit(s) (plus extra credits for completion). Recommended Type of Completion: graded credit. Other types of completion: z (credit).
Teacher(s)
prof. RNDr. Jiří Sopoušek, CSc. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. RNDr. Pavel Brož, Ph.D. (seminar tutor)
doc. Mgr. Jana Pavlů, Ph.D. (seminar tutor)
Mgr. Ondřej Zobač, Ph.D. (assistant)
Guaranteed by
prof. RNDr. Jiří Sopoušek, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Sopoušek, CSc.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C5160/01: Mon 8:00–12:50 C10/213, J. Křivohlávek
C5160/02: Wed 8:00–12:50 C10/213, J. Křivohlávek
C5160/03: Thu 8:00–12:50 C10/213, J. Křivohlávek
C5160/04: Mon 13:00–17:50 C10/213, J. Pavlů
Prerequisites
( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika ) && C4660 Basic Physical Chemistry && NOW( C7777 Handling chemicals )
Basic knowledge to deal with PC. Ability to treat with obtained results correctly from point of view statistics. (confidence interval, linear/non-linear regression,...)
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 48 student(s).
Current registration and enrolment status: enrolled: 0/48, only registered: 0/48, only registered with preference (fields directly associated with the programme): 0/48
fields of study / plans the course is directly associated with
Course objectives
At the end of the course students should be able to: Understand and explain a survey of the basic methods of the experimental physical chemistry with a focus on the areas of equilibrium, calorimetry and kinetics.
Syllabus
  • Exercise list:
  • Cryoscopic determination of molar weight and dimerization constant of benzoic acid;
  • Potentiometric measurement of weak-acid constant;
  • Viscosities of solutions of polymers;
  • Ion selective electrode;
  • Measurement of reaction and solution heat of weak and hard acids;
  • Thermodynamics of Galvanic cell;
  • Measurement of heat of fusion of liquid;
  • Ethanol-water phase diagram assessment;
  • Refraction and permittivity of liquids;
  • Evaluation of extraction and dimerization constants of monochloracetate and acetic acids in benzene-water system;
  • Dissociation constant determination of acid-base indicator;
  • Concentration dependence of molar conductivity of weak and hard electrolytes;
  • Sacharose decomposition in acid solution;
  • Determination of ion transport number;
  • Photometric study of reaction kinetics;
  • Activity coefficient determination of HCl;
  • Absorption isotherm determination in water-carbon powder – methylene blue system;
  • Temperature dependency of oxygen concentration in water;
  • Diffusion coefficient evaluation of ammonia in membrane;
  • Ethylacetate decomposition;
  • Adsorption on liquid gas interface;
  • Critical micellar concentration;
Literature
Teaching methods
Individual laboratory work under supervision.
Assessment methods
Final evaluation - Graded credit. Credit requirements - Delivering and teachers agreed protocols of all completed tasks. Attendance mandatory.
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
Information on completion of the course: Náhradní laboratorní úlohy lze absolvovat jen v semestru.
The course is taught annually.
General note: Vyučují učitelé Ústavu chemie na UKB pavilon A12.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation, Autumn 2012, Autumn 2014, Autumn 2015, Autumn 2016, autumn 2017, Autumn 2018, Autumn 2019, Autumn 2020, autumn 2021, Autumn 2022, Autumn 2023, Autumn 2024.
  • Enrolment Statistics (Autumn 2013, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2013/C5160