C3640 Analytical Chemistry for Biologists - laboratory course

Faculty of Science
Spring 2010
Extent and Intensity
0/3/0. 3 credit(s). Type of Completion: z (credit).
Teacher(s)
Mgr. Jiří Machát, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Ivan Holoubek, CSc.
RECETOX – Faculty of Science
Prerequisites (in Czech)
C1660 Basic Analytical Chemistry
Course Enrolment Limitations
The course is offered to students of any study field.
Course objectives
Basic laboratory course of analytical chemistry will prepare students for work in analytical laboratory and these skills can be applied in furher study. Main objectives of the course can be summarized as follows: to perform qualitative analysis, gravimetric analysis, volumetric analysis (acidimetric, redox and chelatometric). The course will help to understand basics of instrumental analysis and results evaluation.
Syllabus
  • QUALITATIVE ANALYSIS 1. Analytical reactions of kations and anions I. 2. Analytical reactions of kations II. 3. Quantitative analysis - basic operations 4. Gravimetric determination of Fe in pigment as Fe2O3. 5. Iodometric titration. Determination of Vitamin C in pharmaceuticals and fruits. 6. Chelatometry. Determination of Ca and Mg in water and shell. 7. Statistical data evaluation - argentometric determination of chloride in urine. 8. Spectrophotometry. Determination of Fe in natural water. 9. Atomic absorption and emission spectrometry. Determination of Zn and K in multivitamins. 10. Potentiometric and conductimetric titration. Determination of phosphoric acid in Cola beverages.. 11. Determination of beta-carotene in juice by extraction spectrophotometry. 12. Excursion - instrumental methods of analytical chemistry (AAS, AFS, ICP-OES, ICP-MS, XRF, LIBS, MFS, MAS, HPLC, GC, CE, LIF, MALDI-MS etc.).
Literature
  • HOLZBECHER, Záviš. Návody pro laboratorní cvičení z analytické chemie. 3. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 1991, 160 s. ISBN 80-7080-090-9. info
  • FOGL, Jaroslav. Návody pro laboratorní cvičení z analytické chemie. 2. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2000, 1 sv. (rů. ISBN 80-7080-393-2. info
  • KROFTA, Jiří. Návody pro laboratorní cvičení z analytické chemie. 6. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2001, 1 sv. (rů. ISBN 80-7080-451-3. info
  • MATĚJKA, Pavel. Návody pro laboratorní cvičení z analytické chemie. 1. vyd. Praha: Vysoká škola chemicko-technologická, 2002, 1 sv. (rů. ISBN 80-7080-466-1. info
Assessment methods
Final evaluation - credit. Requirements: accurate and teacher reviewed protocols of all completed tasks. Mandatory attendance, 1 absence due to illness accepted.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Spring 2003, Autumn 2003, Spring 2004, Autumn 2004, Spring 2005, Autumn 2005, Spring 2006, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Autumn 2009.
  • Enrolment Statistics (recent)
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