C3640 Analytical Chemistry - laboratory course

Faculty of Science
Autumn 2008
Extent and Intensity
0/3/0. 3 credit(s). Type of Completion: z (credit).
Teacher(s)
prof. RNDr. Přemysl Lubal, Ph.D. (seminar tutor)
Mgr. Jiří Machát, Ph.D. (seminar tutor)
doc. Mgr. Karel Novotný, Ph.D. (seminar tutor)
doc. Mgr. Petr Táborský, Ph.D. (seminar tutor)
Ing. Blanka Vrbková, Ph.D. (seminar tutor)
Guaranteed by
doc. Mgr. Karel Novotný, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C3640/01: Thu 14:00–16:50 C10/209, J. Machát
C3640/03: Mon 8:00–10:50 C10/209, B. Vrbková
C3640/04: Thu 8:00–10:50 C10/209, K. Novotný
C3640/05: Thu 11:00–13:50 C10/209, K. Novotný
C3640/06: Tue 8:00–10:50 C10/209, P. Lubal
Prerequisites (in Czech)
NOW( C1660 Basic Analytical Chemistry ) && NOW( C7777 Handling chemicals )
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Basic laboratory course of analytical chemistry will prepare students for work in analytical laboratory and these skills can be applied in furher study. Main objectives of the course can be summarized as follows: to perform qualitative analysis, gravimetric analysis, volumetric analysis (acidimetric, redox and chelatometric). The course will help to understand basics of instrumental analysis and results evaluation.
Syllabus
  • QUALITATIVE ANALYSIS 1. Analytical reactions of kations and anions I. 2. Analytical reactions of kations II. 3. Quantitative analysis - basic operations 4. Gravimetric determination of Fe in pigment as Fe2O3. 5. Iodometric titration. Determination of Vitamin C in pharmaceuticals and fruits. 6. Chelatometry. Determination of Ca and Mg in water and shell. 7. Statistical data evaluation - argentometric determination of chloride in urine. 8. Spectrophotometry. Determination of Fe in natural water. 9. Atomic absorption and emission spectrometry. Determination of Zn and K in multivitamins. 10. Potentiometric and conductimetric titration. Determination of phosphoric acid in Cola beverages.. 11. Determination of beta-carotene in juice by extraction spectrophotometry. 12. Excursion - instrumental methods of analytical chemistry (AAS, AFS, ICP-OES, ICP-MS, XRF, LIBS, MFS, MAS, HPLC, GC, CE, LIF, MALDI-MS etc.).
Literature
  • HOLZBECHER, Záviš. Návody pro laboratorní cvičení z analytické chemie. 3. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 1991, 160 s. ISBN 80-7080-090-9. info
  • FOGL, Jaroslav. Návody pro laboratorní cvičení z analytické chemie. 2. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2000, 1 sv. (rů. ISBN 80-7080-393-2. info
  • KROFTA, Jiří. Návody pro laboratorní cvičení z analytické chemie. 6. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2001, 1 sv. (rů. ISBN 80-7080-451-3. info
  • MATĚJKA, Pavel. Návody pro laboratorní cvičení z analytické chemie. 1. vyd. Praha: Vysoká škola chemicko-technologická, 2002, 1 sv. (rů. ISBN 80-7080-466-1. info
Assessment methods
Final evaluation - credit. Requirements: accurate and teacher reviewed protocols of all completed tasks. Mandatory attendance, 1 absence due to illness accepted.
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
The course can also be completed outside the examination period.
The course is taught annually.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Spring 2003, Autumn 2003, Spring 2004, Autumn 2004, Spring 2005, Autumn 2005, Spring 2006, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2009, Spring 2010.
  • Enrolment Statistics (Autumn 2008, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2008/C3640