C1600 Laboratory in Chemistry

Faculty of Science
Spring 2012
Extent and Intensity
0/4/0. 4 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
Teacher(s)
Mgr. Miroslava Bittová, Ph.D. (seminar tutor)
Mgr. Aleš Hrdlička, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Guaranteed by
doc. Mgr. Marek Nečas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C1600/01: Tue 8:00–11:50 C10/312, A. Pálková
C1600/02: Tue 13:00–16:50 C10/312, A. Hrdlička
C1600/03: Wed 8:00–11:50 C10/312, M. Petlachová
C1600/04: Thu 8:00–11:50 C10/312, A. Pálková
C1600/05: Thu 13:00–16:50 C10/312, M. Bittová
C1600/06: Mon 15:00–18:50 C10/312, M. Bittová
C1600/07: Fri 8:00–11:50 C10/312, S. Janků
Prerequisites
C7777 Handling chemicals
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 14 fields of study the course is directly associated with, display
Course objectives
At the end of this course, students should be able to: practise basic laboratory operations (filtration, crystallization, distillation, extraction, sublimation, volumetric methods); use basic methods of determination of physicochemical constants of compounds; apply basic chemistry calculations in laboratory praxis.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for laboratory work and writing reports, safety rules. Pass-requirements. 2. Filtration, extration, simple destillation, destillation under reduced pressure, determination of the refractive index 3. Preparation of buffers, pH measurement, izolation of trimyristine from nutmeg 4. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture. 5. Preparation of H2SO4 volumetric solution, volumetric measurement of the molarity, density of the solution 6. Preparation of CuSO4.5H2O 7. Manganometric, chelatometric titration 8. Preparation of Cu(II)comlex 9. Preparation of paracetamol, melting point, TLC 10. Extraction of plant pigmets, preparation of terc-butylchloride 11. Isolation of caffeine from tea leaves 12. Preparation of 2-chlorbenzoic acid
Literature
    recommended literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • MAREČEK, Aleš and Antonín RŮŽIČKA. Laboratorní technika pro nechemické obory. 1. vyd. Brno: Vydavatelství Masarykovy univerzity, 1997, 44 s. ISBN 8021016531. info
Teaching methods
Laboratory course.
Assessment methods
In-term tests to check an understanding of each completed laboratory exercise and related principles and calculations (stoichiometry, concentrations, titrations). Laboratory reports on all exercises.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2024, Spring 2025.
  • Enrolment Statistics (Spring 2012, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2012/C1600