PřF:C8953 NMR Structural Analysis - sem. - Course Information
C8953 NMR Structural Analysis - seminar
Faculty of ScienceSpring 2016
- Extent and Intensity
- 0/2/0. 2 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
- Teacher(s)
- Mgr. Jan Novotný, Ph.D. (seminar tutor)
Mgr. Martin Novák, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Ing. Mgr. Karolina Wawrocka (assistant) - Guaranteed by
- prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Contact Person: Mgr. Jan Novotný, Ph.D.
Supplier department: National Centre for Biomolecular Research – Faculty of Science - Timetable
- Wed 15:00–16:50 C04/211
- Prerequisites
- C8950 NMR Structural Analysis || NOW ( C8950 NMR Structural Analysis )
successful completion/simultaneous registration of C8950 - Course Enrolment Limitations
- The course is also offered to the students of the fields other than those the course is directly associated with.
- fields of study / plans the course is directly associated with
- there are 15 fields of study the course is directly associated with, display
- Course objectives
- At the end of the course students should be able to: analyse and interpret 1D and 2D NMR spectra; solve the structure of an unknown compound based on the spectral analysis.
- Syllabus
- Interpretation: 1. H-1 NMR spectra. 2. C-13 NMR spectra. 3. APT. 4.+5. 1D NOE and NOESY. 6. COSY. 7. TOCSY. 8. HSQC. 9. HMBC. 10.+11. Set of spectra for one sample. 12. Presentation of group project.
- Literature
- recommended literature
- CLARIDGE, Timothy D. W. High-resolution NMR techniques in organic chemistry. 1st ed. Amsterdam: Pergamon, 1999, xiv, 382 s. ISBN 0-08-042798-7. info
- BREITMAIER, Eberhard. Structure elucidation by NMR in organic chemistry : a practical guide. Translated by Julia Wade. Chichester: John Wiley & Sons, 1993, 265 s. ISBN 0471933813. info
- FRIEBOLIN, Horst. Basic one- and two-dimensional NMR spectroscopy. Translated by Jack K. Becconsall. 5th completely rev. and upda. Weinheim: Wiley-VCH, 2011, xxiv, 418. ISBN 9783527327829. info
- BRAUN, Siegmar, Hans-Otto KALINOWSKI and Stefan BERGER. 150 and more basic NMR experiments : a practical course. 2nd exp. ed. Weinheim: Wiley-VCH, 1998, 595 s. ISBN 3527295127. info
- Teaching methods
- Practical exercises in interpreting the NMR spectra; disscussions; group project.
- Assessment methods
- Participation on practical sessions, final project.
- Language of instruction
- Czech
- Follow-Up Courses
- Further Comments
- Study Materials
The course is taught annually.
- Enrolment Statistics (Spring 2016, recent)
- Permalink: https://is.muni.cz/course/sci/spring2016/C8953