C1100k Laboratory techniques

Faculty of Science
Spring 2025
Extent and Intensity
0/0/5. 5 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
In-person direct teaching
Teacher(s)
Světlana Filípková (seminar tutor)
Ing. Mgr. Bc. Radka Kopecká, Ph.D. (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
doc. Mgr. Karel Novotný, Ph.D. (alternate examiner)
Guaranteed by
doc. Mgr. Karel Novotný, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
C7777 Handling chemical substances && C1020 General Chemistry && C1040 General Chemistry-sem.
C7777 Handling with chemicals C1020 Principles of chemistry C1040 Seminary to the course C1020 Theoretical and practical knowledge on secondary school chemistry level, knowledge of gputtinf chemical equations together, stoichiometric concentration a diluting calculations
Course Enrolment Limitations
The course is only offered to the students of the study fields the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Students learn the basic work in a chem. laboratory (filtration, distillation, sublimation), the first aid and rules with chemical handling. Students: - learn basic safety and fire regulations and form a habit for safe laboratory work - learn determinations of simple physico-chemical measurements a their evaluation - are taught about handling with simple chemical apparatuses and learn to operate with them under their safe work - carry out more advanced experiments a learn to make a report containing results, graphs, figures, tables
Learning outcomes
Students will be able to perform the basic tasks in the chemical laboratory independently, assemble the apparatus, synthesize and characterize some substances. The students will be able to evaluate results and write a report.
Syllabus
  • 1. Introduction, laboratory equipment, laboratory and working rules. Work and fire safety organisation od the course, chemicals, pressure bottles, laboratory glass and other materials 2. Filtration under normal and lowered pressure, frita, Büchner funnel. Glass-blower workplace, simple glass-blower works 3. Separation of the mixture Cr2O3+ KAl(SO4)2 + CuSO4.5H2O, Preparation od volumetric NaCl solution, concentration calculations, pycnometric density determination 4., 5. Mounting of simple apparatuses, distillation, Soxhlet extraction, rectification, sublimation apparatus, refractometer, melting point determination, rotary vaccuum evaporator 6. Handling with measuring glass vessels; determination of 0,1M NaOH factor; preparation of approximately 0,5M H2SO4 and alkalimetric determination of its concentration; density determination by using densimeter; determination of atomic relative mass for Al and Mg 7. – 12. Tasks cycling: Preparation of Bi2O3 and metallic Bi by reduction with hydrogen and oxalate Aluminotermic preparation of iron from Fe2O3 Ph measurements using a touch electrode, paper, leather, textile; measurement using immersible electrode - 0,5M NaOH, 0,15M HCl Taking photos Electrode potentials measured by 1st type electrodes, verification of Nernst equation Electrochemical galvanizing of brass electrode by copper, verification of Faraday law Preparation of copper vitriol Determination of chlorides by ion-selective electrode (potentiometry) Conductometric titration, Cl- concentration determination conductometrically Argentometry Distillation of the mixture acetone-toluene using simple distillation apparatus Rectification of the mixture acetone-toluene using Jantzen column Extraction od plant dyes using Sohlet extractor, chromatography, evaporator Preparation of Mohr salt 13. Final testing, substitution of missed courses, glass cleaning, laboratory cleaning.
Literature
  • PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
  • PŘÍHODA, Jiří and Jiří TOUŽÍN. Pomůcka pro seminář z obecné chemie. 1. vyd. Brno: Masarykova univerzita, 2012, 149 s. ISBN 9788021058132. info
Teaching methods
Laboratory course involves training of basic laboratory techniques, calculations and drawing up the report
Assessment methods
Laboratory course takes place every week. Readiness od every student is checked by a short testing or by oral examination. All calculations must be prepared before the course beginning. A student is obliged to have a laboratory book. Missed courses have to be properly excused and it is necessary to do them in alternative time limit. Requirements for gaining credits: a) presence in all courses times b)knowledge of principles and instructions for all excercised tasks, stoichiometric and diluting calculations, titration calculations c)making af single excercise reports d)succsessful execution of the test from laboratory techniques e)paying for laboratory glass apparatuses broken due to own faults
Language of instruction
Czech
Listed among pre-requisites of other courses
The course is also listed under the following terms Spring 2012, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2024.
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