Course Information

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2024

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).
In-person direct teaching

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Students will learn basics of 1D NMR measurement. Students will be able to prepare NMR sample, measure NMR spectra and process data of common nuclei : ¹H, ¹³C, ¹⁹F, ¹¹B, ³¹P at the end of the course.

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2025

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).
In-person direct teaching

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2024

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2023

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2023

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2022

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2022

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
autumn 2021

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2021

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2020

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2020

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

https://is.muni.cz/www/moravec/c7998_zaklady_experimentalni_nmr_spektroskopie/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2019

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Learning outcomes

Student will be able to: - prepare sample for NMR; - select and set NMR experiment; - control measurement during acquisition;

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2019

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2018

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Tomáš Lízal, Ph.D. (seminar tutor)
Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
spring 2018

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
autumn 2017

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2017

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

Mgr. Zdeněk Moravec, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

Inorganic Chemistry (programme PřF, N-CH)
Chemistry (programme PřF, B-CH)
Material Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2016

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2016

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2015

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2014

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2013

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2012

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1020 General Chemistry
Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

At the end of the course students should be able to measure of 1D NMR spectra (1H, 13C, APT) at 300 MHz spectrometer; probehead exchange; temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed in controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F).

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2011

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Mgr. Jan Vícha, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Timetable

Wed 9:00–10:50 Kontaktujte učitele

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2011

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Timetable

Wed 9:00–11:50 Kontaktujte učitele

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2010

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Mgr. Jan Vícha, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Timetable

Tue 9:00–9:50 C04/211

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2010

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Timetable

Wed 9:00–11:50 Kontaktujte učitele

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

At the end of the course students should be able to measure of 1D NMR spectra (1H, 13C, APT) with 300 MHz spectrometer; including replacement of probehead; temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed for controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F).

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2009

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 19 fields of study the course is directly associated with, display

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

Study Materials
The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2009

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Measurements of 1D NMR spectra (1H, 13C, APT) with 300 MHz spectrometer; replacement of probeheadů temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed for controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F).

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2008

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Základy experimentální NMR spektroskopie

Faculty of Science
Spring 2008

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2007

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Základy experimentální NMR spektroskopie

Faculty of Science
Spring 2007

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2006

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2015

The course is not taught in Spring 2015

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2014

The course is not taught in Spring 2014

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

NMR lab introducing
AVANCE 300 MHz NMR spectrometer: construction of cryomagnet
NMR probes
Temperature unit
Hardware and software (TopSpin)
Basics of pulse-field NMR spectrometry:
deuterium stabilization (lock)
tunning of field homogenity (shimming)
acquisition parameters, pulse sequences, FID (Free induction decay)
matemathical operation with FIDs – windows functions Fourier transformation, data processing, phase corrections
Measurement and interpretation of 1H NMR spectra
Measurement of 1H NMR (300 MHz) spectra of unknown compound CDCl3 at 298 and 313 K under operator guidance
1H NMR spectra interpretation: o integral intensity, spin-spin couplings, chemical Shift determinativ and overall structural elucidation
Measurement and interpretation of 13C NMR spectra (APT), 11B and 19F NMR or other nuclei on regest
Measurement of 13C NMR (75MHz) spectra with and withou proton decoupling under operator guidance
APT spectra
Interpretation of 13C and APT NMR spectra
Measurement and interpretation of 11B and 19F NMR spectra of unknown compound.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Practical training

Assessment methods

Full attandance is mandatory. Student has to performed basic NMR experiments (1H, 13C and APT).

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2013

The course is not taught in Spring 2013

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Lukáš Maier, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (alternate examiner)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2012

The course is not taught in Spring 2012

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Supplier department: National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, N-CH)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
spring 2012 - acreditation

The information about the term spring 2012 - acreditation is not made public

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Supplier department: National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://nmrlab.chemi.muni.cz/c7998.php

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2011 - acreditation

The information about the term Autumn 2011 - acreditation is not made public

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Mgr. Jan Vícha, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2010 - only for the accreditation

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Mgr. Jan Vícha, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2011 - only for the accreditation

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Syllabus

1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Probehead exchange, ACD software, interpretation of the NMR spectra, various isotopes - experimental aspects. File transfer.

Literature

recommended literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Teaching methods

Laboratory training

Assessment methods

Practical sessions. Practical exam.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Základy experimentální NMR spektroskopie

Faculty of Science
Spring 2008 - for the purpose of the accreditation

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Autumn 2007 - for the purpose of the accreditation

Extent and Intensity

0/0/1. 1 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science

Prerequisites

Basic knowledge of NMR spectroscopy.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Chemistry (programme PřF, M-CH)
Chemistry (programme PřF, B-CH)
Organic Chemistry (programme PřF, D-CH)
Organic Chemistry (programme PřF, N-CH)
Organic Chemistry (programme PřF, N-CH3)

Course objectives

Základy měření 1D NMR spekter (1H, 13C, APT) na 300 MHz spektrometru. Výměna sondy a teplotní měření. Zpracování a interpretace spekter.

Syllabus (in Czech)

1. NMR spektrometr, software XWin-NMR (TopSpin), měřící sonda, NMR kyveta, příprava vzorku, měření jádra H-1. 2. Základy zpracování NMR spekter, teplotní jednotka, měření jádra C-13, APT experiment. 3. Výměna sondy, ACD software, interpretace spekter, experimentální aspekty měření jiných jader.

Literature

Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5

Assessment methods (in Czech)

Praktická výuka ovladání NMR spektrometru a zpracování dat. Účast na praktickém cvičení nutná.

Language of instruction

Czech

Follow-Up Courses

Further Comments

The course is taught each semester.
The course is taught: in blocks.

Teacher's information

http://www.chemi.muni.cz/nmr/radek/C7998/

The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Spring 2009, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.

Enrolment Statistics (Autumn 2024, recent)

Course Information

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Základy experimentální NMR spektroskopie

C7998 Basics of Experimental NMR Spectroscopy

C7998 Základy experimentální NMR spektroskopie

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Basics of Experimental NMR Spectroscopy

C7998 Základy experimentální NMR spektroskopie

C7998 Basics of Experimental NMR Spectroscopy

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