C6250 Methods of Chemical Research - laboratory

Faculty of Science
Spring 2024
Extent and Intensity
0/0/5. 5 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
Teacher(s)
RNDr. Marta Farková, CSc. (seminar tutor)
Mgr. Aleš Hrdlička, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
doc. Mgr. Petr Táborský, Ph.D. (seminar tutor)
Mgr. Jan Valášek (assistant)
Mgr. Vojtěch Vrána (assistant)
Guaranteed by
RNDr. Marta Farková, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C6250/01: Mon 19. 2. to Sun 26. 5. Mon 8:00–12:50 C10/209, M. Farková, Z. Moravec
C6250/02: Mon 19. 2. to Sun 26. 5. Thu 7:00–11:50 C10/209, M. Farková, Z. Moravec
C6250/03: Mon 19. 2. to Sun 26. 5. Tue 14:00–18:50 C10/209, A. Hrdlička, Z. Moravec
C6250/04: Mon 19. 2. to Sun 26. 5. Tue 8:00–12:50 C10/209, A. Hrdlička, Z. Moravec
Prerequisites (in Czech)
C5190 Instr. Anal. Chem. II-lab. || C7640 Analytical Chem.-lab.course
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
At the end of the course students will know instrumental methods and will be able to process results of the measurements.
Learning outcomes
At the end of the course student will know advanced instrumental methods; will be able to evaluate the results of the measurements; to use appropriate software; to present the results.
Syllabus
  • 1. Orientation tests, qualitative elemental analysis, classification and group reactions, physical constants determination of organic compounds. 2. Semimicrodetermination of carbon and hydrogen. 3. Volumetric determination of nitrogen according to Dumas and Dubsky. 4. Microdetermination of sulfur according to Schöniger. 5. Derivatization of alcohols and their identification by TLC. 6. Interpretation of spectra of organic molecules. 7. Gas chromatography. Determination of alcohols in an alcoholic drink. 8. Capillary electrophoresis. Determination of caffeine and acetylsalicylic acid in Acylcoffin. 9. Liquid chromatography on reverse phase with UV-VIS detection
Literature
    required literature
  • FARKOVÁ, Marta, Blanka VRBKOVÁ and Helena ZAVADILOVÁ. Metody chemického výzkumu – praktikum (Methods of chemical research - laboratory). 1. vyd. Brno: Masarykova univerzita, 2012, 170 pp. mimo edice. ISBN 978-80-210-5783-8. info
    not specified
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin. 1. vyd. Olomouc: Univerzita Palackého, 1981, 235 s. info
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin b. 1. vyd. Olomouc: Univerzita Palackého, 1981, 235 s. info
Teaching methods
Type of education: students have to pass all exercises included in the course
Assessment methods
Type of exam: written tests, final test, oral examination during the lessons. Students have to submit all protocols.
Language of instruction
Czech
Further Comments
Study Materials
The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Spring 2000, Spring 2001, Spring 2002, Spring 2003, Spring 2004, Spring 2005, Spring 2006, Spring 2007, Spring 2008, Spring 2009, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2025.
  • Enrolment Statistics (Spring 2024, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2024/C6250