C1635 Analytical chemistry - laboratory course

Faculty of Science
Autumn 2022
Extent and Intensity
0/3/0. 3 credit(s) (plus extra credits for completion). Type of Completion: z (credit).
Teacher(s)
Mgr. Markéta Holá, Ph.D. (seminar tutor)
prof. RNDr. Přemysl Lubal, Ph.D. (seminar tutor)
doc. Mgr. Karel Novotný, Ph.D. (seminar tutor)
doc. Mgr. Petr Táborský, Ph.D. (seminar tutor)
doc. RNDr. Jiří Urban, Ph.D. (seminar tutor)
doc. Mgr. Tomáš Vaculovič, Ph.D. (seminar tutor)
Guaranteed by
doc. Mgr. Tomáš Vaculovič, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Timetable of Seminar Groups
C1635/01: Mon 8:00–10:50 C10/207, P. Táborský
C1635/02: Thu 9:00–11:50 C10/207, T. Vaculovič
Prerequisites (in Czech)
NOW( C1660 Basic Analytical Chemistry )|| C1660 Basic Analytical Chemistry
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Basic laboratory course of analytical chemistry will prepare students for work in analytical laboratory and these skills can be applied in further study. Main objectives of the course can be summarized as follows: to perform qualitative analysis, gravimetric analysis, volumetric analysis (acidimetric, redox and chelatometric). The course will help to understand basics of instrumental analysis and results evaluation.
Learning outcomes
The student will be able to do titration and gravimetric determination of various analytes and evaluate the results obtained by fundamental analytical instrumental methods.
Syllabus
  • QUALITATIVE ANALYSIS 1. Analytical reactions of cations and anions I. 2. Analytical reactions of cations II. 3. Quantitative analysis - basic operations 4. Gravimetric determination of Fe in pigment as Fe2O3. 5. Iodometric titration. Determination of Vitamin C in pharmaceuticals and fruits. 6. Chelatometry. Determination of Ca and Mg in water and shell. 7. Statistical data evaluation - argentometric determination of chloride in urine. 8. Spectrophotometry. Determination of Fe in natural water. 9. Atomic absorption and emission spectrometry. Determination of Zn and K in multivitamins. 10. Potentiometric and conductimetric titration. Determination of phosphoric acid in Cola beverages.. 11. Determination of beta-carotene in juice by extraction spectrophotometry. 12. Excursion - instrumental methods of analytical chemistry (AAS, AFS, ICP-OES, ICP-MS, XRF, LIBS, MFS, MAS, HPLC, GC, CE, LIF, MALDI-MS etc.).
Literature
  • HOLZBECHER, Záviš. Návody pro laboratorní cvičení z analytické chemie. 3. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 1991, 160 s. ISBN 80-7080-090-9. info
  • FOGL, Jaroslav. Návody pro laboratorní cvičení z analytické chemie. 2. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2000, 1 sv. (rů. ISBN 80-7080-393-2. info
  • KROFTA, Jiří. Návody pro laboratorní cvičení z analytické chemie. 6. přeprac. vyd. Praha: Vysoká škola chemicko-technologická, 2001, 1 sv. (rů. ISBN 80-7080-451-3. info
  • MATĚJKA, Pavel. Návody pro laboratorní cvičení z analytické chemie. 1. vyd. Praha: Vysoká škola chemicko-technologická, 2002, 1 sv. (rů. ISBN 80-7080-466-1. info
Teaching methods
laboratory experiments
Assessment methods
Final evaluation - credit. Requirements: accurate and teacher reviewed protocols of all completed tasks. Mandatory attendance, 1 absence due to illness accepted. Short test is written in each laboratory course. Minimal percentage of these tests is 60 %.
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
The course can also be completed outside the examination period.
The course is taught annually.
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Autumn 2016, autumn 2017, Autumn 2018, Autumn 2019, Autumn 2020, autumn 2021, Autumn 2023, Autumn 2024.
  • Enrolment Statistics (Autumn 2022, recent)
  • Permalink: https://is.muni.cz/course/sci/autumn2022/C1635