PřF:C7998 Basics of Experimental NMR Spe - Course Information
C7998 Basics of Experimental NMR Spectroscopy
Faculty of ScienceAutumn 2008
- Extent and Intensity
- 0/0/1. 1 credit(s). Type of Completion: z (credit).
- Teacher(s)
- Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor) - Guaranteed by
- prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science - Prerequisites
- Basic knowledge of NMR spectroscopy.
- Course Enrolment Limitations
- The course is also offered to the students of the fields other than those the course is directly associated with.
- fields of study / plans the course is directly associated with
- Chemistry (programme PřF, M-CH)
- Chemistry (programme PřF, B-CH)
- Organic Chemistry (programme PřF, N-CH)
- Course objectives
- Measurements of 1D NMR spectra (1H, 13C, APT) with 300 MHz spectrometer; replacement of probeheadů temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed for controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F). - Syllabus
- 1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.
- Literature
- Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
- Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5
- Assessment methods
- Practical sessions. Practical exam.
- Language of instruction
- Czech
- Follow-Up Courses
- Further Comments
- The course is taught each semester.
The course is taught: in blocks. - Teacher's information
- http://www.chemi.muni.cz/nmr/radek/C7998/
- Enrolment Statistics (Autumn 2008, recent)
- Permalink: https://is.muni.cz/course/sci/autumn2008/C7998